Lab Scale 5T Spark Plasma Sintering Hot Press Furnace SPS System

Contact Person:Gilia Ding


Email: gilia@inthelaboratory.com

Tel:+86 177 5900 4070
Telephone:+86-177-59004070
Whatsapp: +86 177 5900 4070
Wechat:Dingqiuna



  • Item no.:

    LITH-SPS-5T-40-mini
  • Payment:

    L/C, T/T, Western Union, Credit Cards, Paypal
  • Lead Time:

    7 days
  • Compliance:

    CE Certified
  • Warranty:

    Two years limited standard warranty
Categories
  • Product Detail

Lab Scale 5T Spark Plasma Sintering Hot Press Furnace SPS System


 

Introduction

Spark Plasma Sintering (SPS) is a new powder metallurgy sintering technology in which metal or other powder is placed into a mold made of graphite or other materials, and specific sintering power and pressing pressure are applied through the upper/lower punches and current-carrying electrodes. The process completes high-performance materials through discharge activation, thermoplastic deformation, and cooling. SPS features sintering under pressure. The plasma generated by the pulsed current and the applied pressure during sintering help reduce the sintering temperature of the powder. At the same time, the low-voltage, high-current characteristics enable rapid densification of the powder.

Advantages: fast heating rate, short sintering time, low sintering temperature, uniform grain size, good control of fine microstructure, high density of the obtained material, simple operation, high reproducibility, safe and reliable, space saving, energy saving, and low cost.

 

Technical parameters

Parameter

Description

Model


SPS-5T-40-mini

Principle

SPS technology applies ON-OFF DC pulses generated by a special power control unit to the powder sample. In addition to the usual sintering promotion effects of electrical discharge machining (discharge impact pressure and Joule heating), it also effectively utilizes the spark discharge phenomenon (instantaneous hightemperature plasma) between powder particles at the initial stage of the pulse discharge to promote sintering, achieving rapid densification through an instantaneous high-temperature field.

Advantages

1. Large chamber space, easy operation.
2. The upper and lower punches are equipped with thermocouples for temperature detection. If any abnormality occurs, the user will immediately observe it and can shut down the equipment to prevent damage.
3. Infrared pyrometer measures temperature from the top of the furnace, which is more accurate than side measurement.
4. The water cooling system has water temperature and water pressure monitoring. In case of abnormality, an alarm is triggered and heating is automatically cut off.
5. Equipped with an explosion protection system. When the pressure inside the chamber exceeds the set value, an alarm is triggered and heating is cut off.
6. Provides overtemperature, overpressure, overcurrent, undervoltage, broken thermocouple protection and indication.

Power

42 KW (Power supply 40 KW + Mechanical pump 1.1 KW + others)

Punch Diameter

80 mm

Power Supply Voltage

Threephase, 380V

Pulse Power Supply

QQ20260527-101544.jpg

(Image reference)
High-stability pulse output: pulse train period and conduction width are uniform, no waveform distortion or phase shift, indicating precise power control logic and long-term stable output of set current.
Excellent synchronization: load current (yellow channel) and voltage (purple channel) signals are fully phase-synchronized with negligible response delay, ensuring simultaneous Joule heating and plasma effects during sintering.
High-frequency carrier characteristics: carrier frequency stable at approx. 30.86 kHz, steep current rise edge, quickly forming uniform discharge paths between powder particles for efficient sintering.
Clean turn-off characteristics: no tailing or freewheeling during current turnoff, accurately controlling single-pulse energy and avoiding ineffective heating or local overheating.

SPS Power Supply

Power

40 kVA

Input Voltage

Three-phase five-wire AC380V/50Hz

Output Current (instantaneous)

DC 0-4000 A

Output Voltage (instantaneous)

DC 0-10 V (rectangular wave peak)

Pulse Parameters

On-time: 1-255 ms
Off-time: 1-255 ms
Pulse count: 1-255 ms
Dwell time: 3-255 ms

Control System

20221018-10.png

The control system consists of a PLC program and a touch screen. The touch screen integrates the company’s proprietary control system. All operations are integrated into the touch screen – user-friendly interface, one-button operation, simple and convenient.

Chamber Vacuum Degree (with molecular pump unit)

< 6×10⁻⁴ Pa

Chamber Gas Filling Pressure

< 0.05 MPa

Pressure Rise Rate

<4 Pa/hour

Chamber Interior View

SPS-QT.jpg

Broken Thermocouple Protection & Indication

Yes

Over-temperature Protection

Yes

Over-current Protection

Yes

Under-voltage Protection (Water Pressure)

Yes

Temperature Control Mode

Intelligent PID

Temperature Control Accuracy

±1°C

Temperature Measurement Methods

TungstenRhenium thermocouple and infrared pyrometer.
TungstenRhenium thermocouple range: 0–1800°C.
Imported infrared pyrometer range: 600–3000°C.

Infrared Pyrometer

QQ20260527-101618.jpg

Japan Chino IRCZ H7T is a highend, ultrahigh temperature fiberoptic infrared pyrometer. Its notable feature is a robust probe consisting of a sapphire lens and optical fiber, which transmits infrared radiation energy to a rear converter for processing.
Spectral response: typically short wavelength 0.9–1.55 μm, ideal for measuring hightemperature, bright or polished metal surfaces (e.g., molten steel, stainless steel, tungsten, molybdenum), as well as silicon crystals, graphite, etc. It maintains good measurement performance even at low emissivity.
Twocolor infrared pyrometer, range 600–3000°C.
Strong antiinterference, unaffected by electromagnetic interference.
High measurement accuracy: below 1000°C: ±5°C; 1000–1500°C: ±0.5% of reading; 1500–2500°C: ±0.6% of reading; above 2500°C: ±1% of reading.

Observation Window Size

Yes (provided)

Pressing System

Electric input method. Hydraulic station with imported proportional valve, potentiometer, pressure sensor, displacement display using a grating ruler (accuracy 0.02 mm), hydraulic cylinder and related hydraulic devices. Pressure adjustment can be switched between manual and automatic, and can be adjusted manually. Automatic pressure adjustment can be set via the touch screen, with stable pressure holding capability.

f976b1beda7a6ef84e75f9257e1b045.jpg

Temperature Control Instrument

Eurotherm 3504 programmable temperature controller.
1. Highprecision temperature instrument, LCD display, 5digit display, simple configuration via quick setup, °C/°F switching.
2. 500segment program control, 8 groups of PID intelligent adjustment.
3. Overtemperature protection and broken thermocouple protection – when overtemperature or thermocouple break occurs, the furnace heating circuit is automatically cut off (when the furnace temperature exceeds 1820°C or the thermocouple burns out, the AC relay on the main circuit automatically disconnects, the main circuit is cut off, the ON lamp on the panel goes out, the OFF lamp lights up, effectively protecting the furnace).
4. Supports various communication interfaces: Modbus, Ethernet, Profibus, Devicenet – can be integrated with any PLC or upperlevel system.
5. Poweroff protection: after power failure and restart, the program does not start from the initial temperature but from the furnace temperature at the time of power failure.
6. The instrument has an autotuning function.

3504-34-500x500.jpg

Graphite Mold

1. The hightemperature mold unit is made of highpurity graphite. Maximum working pressure: 50 MPa.
2. Carefully design the dimensions of the hightemperature mold and select the correct pressure.

Pressure Control

PID program control

Punch Stroke

100 mm

Maximum Temperature

For 10 mm material: 2300°C
For 15 mm material: 2000°C
For 20 mm material: 1700°C

Pressing Pressure Accuracy

±1 kg

Maximum Pressure

5 T

Water Cooling System

Composed of pipes and related devices. Cooling water enters the main inlet, then is distributed through branches to the furnace body, furnace cover, furnace bottom, watercooled electrodes, and other points requiring cooling, then collected and discharged. Cooling water circulation hoses are made of hightemperatureresistant rubber. The main inlet pipe is equipped with an electric contact pressure gauge – when water pressure drops below 0.2 MPa, heating is automatically cut off. The main outlet pipe is equipped with a temperature sensor – when the temperature exceeds 45°C, heating is automatically cut off.

621758b1b1fdecce4e28d2a57bf6541 副本.jpg

Vacuum Pump Unit

Parameter

Specification

Unit Input Voltage

380V / 220V

Bellows

KF40×1000

Vacuum Gate Valve

KF40

Fore Vacuum Pump BSV30

QQ20260527-101907.jpg

Power

1.1 KW

Voltage

380V

Speed

1450 rpm

Inlet Port Diameter

KF25/KF40

Pumping Speed (fore pump)

8 L/s

Ultimate Pressure

5×10⁻¹ Pa

Compound Vacuum Gauge

20190820.jpg

Model

ZDF

Power Supply

220V, 55W

Control Accuracy

±1%

Measuring Range

10⁻⁵ Pa ~ 10⁵ Pa

Secondary Pump – Molecular Pump (can achieve chamber vacuum <6×10⁻⁴ Pa)

QQ20260527-101930.jpg

Molecular Pump Model

FJ620

Input Voltage

220V

Molecular Pump Inlet Flange

DN160

Pumping Speed (for air)

600 L/s

Ultimate Pressure (Molecular Pump)

6×10⁻⁷ Pa

Cooling Method

Water cooling

Cooling Water Pressure

0.1–0.2 MPa

Cooling Water Temperature

<25°C

Ambient Temperature

0–40°C

Recommended Starting Pressure

<10 Pa

Secondary Pump – Diffusion Pump (Optional) (can achieve chamber vacuum <5×10⁻³ Pa)

Voltage

220V

Power

1000 W

Ultimate Vacuum (no leakage)

10⁻⁵ Pa

Inlet Port

DN150

Outlet Port

DN40

Oil Charge

0.3 L

Pumping Speed (N₂)

1000 L/s

Chiller (Optional) – Model HZ-06A

QQ20260527-101939.jpg

Parameter

Specification

Power Supply

3PH380V/50Hz

Total Input Power

8 KW

Maximum Head

30 m

Chilled Water Flow

2.8 m³/h

Tank Capacity

110 L

Cooling Capacity

13244 Kcal/h

Water Inlet/Outlet Port

Rp 1/2"

Machine Dimensions

1300 × 650 × 1145 mm (L×W×H)

 




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