Lab Scale 5T Spark Plasma Sintering Hot Press Furnace SPS System
Introduction
Spark Plasma Sintering (SPS) is a new powder metallurgy sintering technology in which metal or other powder is placed into a mold made of graphite or other materials, and specific sintering power and pressing pressure are applied through the upper/lower punches and current-carrying electrodes. The process completes high-performance materials through discharge activation, thermoplastic deformation, and cooling. SPS features sintering under pressure. The plasma generated by the pulsed current and the applied pressure during sintering help reduce the sintering temperature of the powder. At the same time, the low-voltage, high-current characteristics enable rapid densification of the powder.
Advantages: fast heating rate, short sintering time, low sintering temperature, uniform grain size, good control of fine microstructure, high density of the obtained material, simple operation, high reproducibility, safe and reliable, space saving, energy saving, and low cost.
Technical parameters
|
Parameter |
Description |
|
Model |
SPS-5T-40-mini |
|
Principle |
SPS technology applies ON-OFF DC pulses generated by a special power control unit to the powder sample. In addition to the usual sintering promotion effects of electrical discharge machining (discharge impact pressure and Joule heating), it also effectively utilizes the spark discharge phenomenon (instantaneous hightemperature plasma) between powder particles at the initial stage of the pulse discharge to promote sintering, achieving rapid densification through an instantaneous high-temperature field. |
|
Advantages |
1. Large chamber space, easy operation. |
|
Power |
42 KW (Power supply 40 KW + Mechanical pump 1.1 KW + others) |
|
Punch Diameter |
80 mm |
|
Power Supply Voltage |
Threephase, 380V |
|
Pulse Power Supply |
(Image reference) |
|
SPS Power Supply |
|
|
Power |
40 kVA |
|
Input Voltage |
Three-phase five-wire AC380V/50Hz |
|
Output Current (instantaneous) |
DC 0-4000 A |
|
Output Voltage (instantaneous) |
DC 0-10 V (rectangular wave peak) |
|
Pulse Parameters |
On-time: 1-255 ms |
|
Control System
|
The control system consists of a PLC program and a touch screen. The touch screen integrates the company’s proprietary control system. All operations are integrated into the touch screen – user-friendly interface, one-button operation, simple and convenient. |
|
Chamber Vacuum Degree (with molecular pump unit) |
< 6×10⁻⁴ Pa |
|
Chamber Gas Filling Pressure |
< 0.05 MPa |
|
Pressure Rise Rate |
<4 Pa/hour |
|
Chamber Interior View |
|
|
Broken Thermocouple Protection & Indication |
Yes |
|
Over-temperature Protection |
Yes |
|
Over-current Protection |
Yes |
|
Under-voltage Protection (Water Pressure) |
Yes |
|
Temperature Control Mode |
Intelligent PID |
|
Temperature Control Accuracy |
±1°C |
|
Temperature Measurement Methods |
TungstenRhenium thermocouple and infrared pyrometer. |
|
Infrared Pyrometer
|
Japan Chino IRCZ H7T is a highend, ultrahigh temperature fiberoptic infrared pyrometer. Its notable feature is a robust probe consisting of a sapphire lens and optical fiber, which transmits infrared radiation energy to a rear converter for processing. |
|
Observation Window Size |
Yes (provided) |
|
Pressing System |
Electric input method. Hydraulic station with imported proportional valve, potentiometer, pressure sensor, displacement display using a grating ruler (accuracy 0.02 mm), hydraulic cylinder and related hydraulic devices. Pressure adjustment can be switched between manual and automatic, and can be adjusted manually. Automatic pressure adjustment can be set via the touch screen, with stable pressure holding capability.
|
|
Temperature Control Instrument |
Eurotherm 3504 programmable temperature controller.
|
|
Graphite Mold |
1. The hightemperature mold unit is made of highpurity graphite. Maximum working pressure: 50 MPa. |
|
Pressure Control |
PID program control |
|
Punch Stroke |
100 mm |
|
Maximum Temperature |
For 10 mm material: 2300°C |
|
Pressing Pressure Accuracy |
±1 kg |
|
Maximum Pressure |
5 T |
|
Water Cooling System |
Composed of pipes and related devices. Cooling water enters the main inlet, then is distributed through branches to the furnace body, furnace cover, furnace bottom, watercooled electrodes, and other points requiring cooling, then collected and discharged. Cooling water circulation hoses are made of hightemperatureresistant rubber. The main inlet pipe is equipped with an electric contact pressure gauge – when water pressure drops below 0.2 MPa, heating is automatically cut off. The main outlet pipe is equipped with a temperature sensor – when the temperature exceeds 45°C, heating is automatically cut off.
|
Vacuum Pump Unit
|
Parameter |
Specification |
|
Unit Input Voltage |
380V / 220V |
|
Bellows |
KF40×1000 |
|
Vacuum Gate Valve |
KF40 |
|
Fore Vacuum Pump BSV30
|
|
|
Power |
1.1 KW |
|
Voltage |
380V |
|
Speed |
1450 rpm |
|
Inlet Port Diameter |
KF25/KF40 |
|
Pumping Speed (fore pump) |
8 L/s |
|
Ultimate Pressure |
5×10⁻¹ Pa |
|
Compound Vacuum Gauge
|
|
|
Model |
ZDF |
|
Power Supply |
220V, 55W |
|
Control Accuracy |
±1% |
|
Measuring Range |
10⁻⁵ Pa ~ 10⁵ Pa |
|
Secondary Pump – Molecular Pump (can achieve chamber vacuum <6×10⁻⁴ Pa)
|
|
|
Molecular Pump Model |
FJ620 |
|
Input Voltage |
220V |
|
Molecular Pump Inlet Flange |
DN160 |
|
Pumping Speed (for air) |
600 L/s |
|
Ultimate Pressure (Molecular Pump) |
6×10⁻⁷ Pa |
|
Cooling Method |
Water cooling |
|
Cooling Water Pressure |
0.1–0.2 MPa |
|
Cooling Water Temperature |
<25°C |
|
Ambient Temperature |
0–40°C |
|
Recommended Starting Pressure |
<10 Pa |
|
Secondary Pump – Diffusion Pump (Optional) (can achieve chamber vacuum <5×10⁻³ Pa) |
|
|
Voltage |
220V |
|
Power |
1000 W |
|
Ultimate Vacuum (no leakage) |
10⁻⁵ Pa |
|
Inlet Port |
DN150 |
|
Outlet Port |
DN40 |
|
Oil Charge |
0.3 L |
|
Pumping Speed (N₂) |
1000 L/s |
Chiller (Optional) – Model HZ-06A
|
Parameter |
Specification |
|
Power Supply |
3PH380V/50Hz |
|
Total Input Power |
8 KW |
|
Maximum Head |
30 m |
|
Chilled Water Flow |
2.8 m³/h |
|
Tank Capacity |
110 L |
|
Cooling Capacity |
13244 Kcal/h |
|
Water Inlet/Outlet Port |
Rp 1/2" |
|
Machine Dimensions |
1300 × 650 × 1145 mm (L×W×H) |







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Email : gilia@inthelaboratory.com









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